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The crude residue was purified by silica gel flash column chromatography ( n -heptane:EtOAc, 2:1) yielding 4-nitrophenyl (2-(pyridin-2-yldisulfaneyl)ethyl) carbonate (89%)
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4 Thirty-aptamer signature of semaglutide treatment in STEP 1 (a) and STEP 2 (b)
